Appro LC-7451 Instruções de Operação Página 6
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UltiMate 3000 Series:
VWD-3100 and VWD-3400RS Variable Wavelength Detectors
Page ii Operating Instructions
3.5.2 Installing the Detector ...................................................................................... 43
3.5.3 Configuring the Detector ................................................................................. 44
3.6 Setting Up the Detector in DCMSLink .................................................................... 48
4 Preparation for Operation (Startup) ........................................................................ 49
4.1 Overview of Actions ................................................................................................ 49
4.2 General Precautions for Connecting Capillaries ...................................................... 50
4.3 Connecting Drain Tubing......................................................................................... 51
4.4 Equilibrating the System .......................................................................................... 52
5 Operation and Maintenance ...................................................................................... 55
5.1 Power-Up ................................................................................................................. 56
5.2 Status Screens .......................................................................................................... 57
5.3 Detector Control ....................................................................................................... 58
5.3.1 Operation from the Front Panel Display .......................................................... 58
5.3.2 Chromeleon Software ...................................................................................... 58
5.4 Display Screens (Function Keys and Menus) .......................................................... 64
5.4.1 Showing the Function Keys ............................................................................. 64
5.4.2 Detector Menus ................................................................................................ 66
5.5 Information for Operating the Detector ................................................................... 73
5.5.1 General Notes ................................................................................................... 73
5.5.2 Setting the Wavelengths................................................................................... 78
5.5.3 Turning on the Lamps ...................................................................................... 78
5.5.4 Monitoring the Lamp Intensity ........................................................................ 79
5.5.5 Starting and Stopping Data Acquisition........................................................... 80
5.5.6 Setting the Display Mode ................................................................................. 82
5.5.7 Leak Detection ................................................................................................. 82
5.5.8 Recording the Temperature Signals ................................................................. 83
5.5.9 Adjusting the Screen Brightness and Contrast ................................................. 83
5.5.10 SmartStartup and SmartShutdown ............................................................... 83
5.6 Special Functions in Chromeleon ............................................................................ 84
5.6.1 Optimizing the Detector Performance ............................................................. 84
5.6.2 Recording Absorbance Spectra ........................................................................ 88
5.6.3 Predictive Performance .................................................................................... 89
5.6.4 Detector Diagnostics ........................................................................................ 90
5.6.5 Operational Qualification and Performance Qualification .............................. 91
5.7 Shutting Down the Detector ..................................................................................... 92
5.8 Routine and Preventive Maintenance ...................................................................... 94
6 Troubleshooting .......................................................................................................... 95
6.1 Overview .................................................................................................................. 95
6.2 Messages on the Detector Display ........................................................................... 96
6.3 Chromeleon Diagnostics Messages ....................................................................... 104
6.4 Operating Problems................................................................................................ 109
- Thermo Scientific Dionex 1
- UltiMate 3000 Series 1
- Operating Instructions 2
- Declaration of Conformity 3
- Table of Content 5
- 1 Introduction 9
- UltiMate 3000 Series: 10
- 1.2 Safety 11
- 1.3 Intended Use 21
- 2 Overview 25
- 2.2 Operating Principle 26
- 2.3 Configurations 28
- 2.4 Interior Components 30
- 2.5 Front Panel Elements 31
- 2.6 Rear Panel 32
- Fig. 5: DAC Board 33
- 2.7 Fluid Connections 35
- 2.8 Flow Cells 36
- 2.9 Lamps 37
- 2.10 Leak Sensor 38
- 2.11 Detector Control 38
- 3 Installation 41
- Shipping locks 42
- Cardboard 42
- 3.4 Connecting the Detector 45
- Guide bar 47
- USB Port 47
- Fig. 13: General page 52
- Fig. 14: Detector page 53
- 4.1 Overview of Actions 57
- 4.3 Connecting Drain Tubing 59
- 5 Operation and Maintenance 63
- 5.1 Power-Up 64
- Wavelength [nm] 65
- 5.3 Detector Control 66
- Fig. 18: Commands dialog box 68
- Fig. 23: Detector menus 74
- 5.4.2.4 Preferences Menu 78
- 89
- 6 Troubleshooting 103
- Dark Current Test failed 113
- Filter Motor Test failed 113
- 6.4 Operating Problems 117
- 7 Service 123
- 7.3 Lamp 127
- 7.4 Flow Cell 133
- Locating pin 137
- 7.5 Drying the Leak Sensor 139
- 8 Technical Information 143
- 9.1 Standard Accessories 147
- 9.2 Optional Accessories 148
- 10 Appendix 153
- 10.2 Digital I/O 155
- Holmium Oxide Glass Filter 156
- 11 Index 157
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